LaS(Se)-TaS2(Se) Misfit Nanotube Formula: LaS(Se)-TaS₂(Se) Core Loss

Submitted by Luc Lajaunie, January 15, 2018.

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Spectrum Metadata

Specimen Name: FEI Titan Low-Base
Spectrum Type: Core Loss
Specimen Formula: LaS(Se)-TaS₂(Se)
Data Range: 524.83 eV - 2008.05 eV
Elemental Edges: Se_L2,3, Se_L1, La_M4,5, Ta_M4,5

Microscope Name / Model: FEI Titan Low-Base
Gun Type: X-FEG
Incident Beam Energy: 200 kV
Resolution: 2 eV
Monochromated: No
Dispersion: 0.726 eV/pixel
Acquisition Mode: stem
Convergence Semi-angle: 18 mrad
Collection Semi-angle: 25 mrad
Detector: Gatan Tridiem ESR 865

Dark Current Correction: No
Gain Variation Spectrum: No
Calibration: low loss + drift tube
Reference: Luc Lajaunie, Gal Radovsky, Reshef Tenne, Raul Arenal (2017). Quaternary Chalcogenide-Based Misfit Nanotubes LnS(Se)-TaS(Se)2 (Ln = La, Ce, Nd, and Ho): Synthesis and Atomic Structural Studies Inorganic Chemistry
DOI: 10.1021/acs.inorgchem.7b02680
Reference URL: http://dx.doi.org/10.1021/acs.inorgchem.7b02680